CN105622060A - Energy ceramic - Google Patents
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- CN105622060A CN105622060A CN201610019217.6A CN201610019217A CN105622060A CN 105622060 A CN105622060 A CN 105622060A CN 201610019217 A CN201610019217 A CN 201610019217A CN 105622060 A CN105622060 A CN 105622060A
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
- C04B33/138—Waste materials; Refuse; Residues from metallurgical processes, e.g. slag, furnace dust, galvanic waste
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/24—Manufacture of porcelain or white ware
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3217—Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3418—Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3436—Alkaline earth metal silicates, e.g. barium silicate
- C04B2235/3445—Magnesium silicates, e.g. forsterite
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Abstract
The invention relates to energy ceramic. The energy ceramic is formed by mixing multiple mineral materials according to an appropriate ratio. Under the synergistic effect of the components, magnetic field energy with appropriate strength can be radiated, the radiated magnetic field energy is matched with magnetic field of a human body, biomagnetic effect is produced inside the human body, various unbalanced or abnormal functional states in the human body can be adjusted and balanced, blood gas circulation of the human body is promoted, blood vessels are unobstructed, and especially pains on neck, shoulders, waist, legs and joints and pains, caused by various reasons, of the human body can be rapidly stopped; and immunity of the human body can be beneficially improved, physical and mental harmony is improved, a person can be full of spirit, happy and energetic, and the energy ceramic provided by the invention has the advantages of high strength, low water absorption, good wear resistance, good shock resistance and the like and has great market value.
Description
Technical field
The invention belongs to magnetic therapy technical field, be specifically related to a kind of energy ceramic.
Background technology
Magnetic is one of thing qualitative attribution. Human body also has certain magnetic, it has now been found that the current active of human brain, heart, skin and other organs has all produced magnetic field, and even the hair follicle on hair has also produced magnetic field. In recent years due to modern magnetics and biological development, occurring in that these boundary science of biomagnetism, now known that biological physiological function is all had certain effect and affects by magnetisable material and magnetic field, this role and influence are biological magnetic effect. This magnetic effect is owing to the electron motion of interior of articles microstructure and the changing of magnetism of composition biological tissue determine. Scientific experiments is it has proven convenient that biological molecule, cell, nerve, organ and the at all levels of whole live body are all demonstrated different impacts by magnetisable material and magnetic field. Magnetic therapy is exactly utilize this biomagnetic effect of inside of human body to adjust and recover various uneven in human body or abnormal functional status to reach the purpose of health care.
" magnetotherapy " is commonly used by medical matters circle already, and it can cause a series of change such as human nerve, body fluid metabolic. There is invigorating blood circulation, change the effects such as silt, detumescence, pain relieving, antiinflammatory, analgesia. Through the development of the medical science of several thousand, magnetic therapy has been had deeper of understanding by recent domestic medical expert, not only applying a magnetic field treatment disease, and applying a magnetic field is as a kind of health means, and magnetic health-care articles for use just arise at the historic moment. But, currently there are magnetic health-care articles for use, it is impossible to concentrating energy, magnetic effect is more weak, and curative effect is very micro-.
Summary of the invention
In order to solve the problems referred to above that prior art exists, the invention provides a kind of magnetic effect energy ceramic obvious, eutherapeutic. Described energy ceramic can be in harmonious proportion human magnetic field, strengthens the circulation of human body vim and vigour, increases body immunity, promotes the mediation of body and mind.
The technical solution adopted in the present invention is:
A kind of energy ceramic, raw material components includes: quartz sand 40-60 weight portion, nine eyestone shale 30-50 weight portions, magnetic iron ore 20-40 weight portion, tourmaline 20-40 weight portion, far-infrared ceramic 15-45 weight portion, white clay 15-25 weight portion, Maifanitum 20-40 weight portion, kerosene shale ash 15-25 weight portion, serpentine 15-45 weight portion, olivine 15-45 weight portion, tufa stone 15-45 weight portion, Kaolin 15-45 weight portion, bauxite 20-40 weight portion, red mud 15-45 weight portion, slag micro powder 20-40 weight portion, and catalyst gives up agent 15-45 weight portion.
It is preferred that the raw material components of described energy ceramic includes: quartz sand 50 weight portion, nine eyestone shale 40 weight portions, magnetic iron ore 30 weight portion, tourmaline 30 weight portion, far-infrared ceramic 25 weight portion, white clay 20 weight portion, Maifanitum 30 weight portion, kerosene shale ash 20 weight portion, serpentine 30 weight portion, olivine 25 weight portion, tufa stone 30 weight portion, Kaolin 30 weight portion, bauxite 30 weight portion, red mud 28 weight portion, slag micro powder 30 weight portion, catalyst gives up agent 28 weight portion.
The useless agent of described catalyst is one or more in methanol-fueled CLC copper zinc dead catalyst, low-temperature conversion copper zinc dead catalyst, aldehyde Hydrogenation alcohol copper zinc dead catalyst.
A kind of method preparing described energy ceramic, comprises the steps:
(1) weigh serpentine, olivine, tufa stone, Kaolin, bauxite, red mud and be sufficiently mixed, obtaining the first mixed material;
(2) described first mixed material is first carried out being warming up to 780-880 DEG C, be incubated 1-2h, then be cooled to 350-400 DEG C, be incubated 4-6h, afterwards successively through shrend, pulverizing, dry, obtain the first premix material, stand-by;
(3) weigh quartz sand, nine eyestone shale, magnetic iron ore, tourmaline, far-infrared ceramic, white clay, Maifanitum and be sufficiently mixed, obtaining the second mixed material;
(4) described second mixed material is first pulverized, obtain fine powder, add water in described fine powder and make serosity, and the pH with the acid solution described serosity of adjustment is 4-5, afterwards described serosity is ground at 70-80 DEG C of temperature 20-30min, then the pH with the alkali liquor described serosity of adjustment is neutral, spray-dried, obtain the second premix material, stand-by;
(5) described for step (2) the first premix material, described second premix material of step (4) are mixed homogeneously with remaining raw material, obtain the 3rd mixed material, waterglass is added in described 3rd mixed material, the addition of described waterglass is equivalent to the 4-8wt% of described 3rd mixed material weight, it is uniformly mixed, repressed molding, dry obtains dry body;
(6) first carry out step (3) described dry body being warming up to 980-1060 DEG C for the first time, insulation 5-8h, carry out again being cooled to 720-780 DEG C for the first time, be incubated 3-4h, carry out second time afterwards again and be warming up to 1160-1220 DEG C, insulation 8-12h, it is cooled to 550-600 DEG C again, is incubated 2-3h, is cooled to room temperature, through edging, obtain described energy ceramic.
In step (2), described temperature-rise period is: first by described first mixed material with the ramp of 4-8 DEG C/min to 450-550 DEG C, be incubated 2-5h, then with the ramp of 2-4 DEG C/min to 780-880 DEG C;
The rate of temperature fall of described temperature-fall period is 5-10 DEG C/min.
In step (2), the particle diameter of described first premix material is 150-200 order.
In step (4), the particle diameter of described fine powder is 200-300 order, and the concentration of described serosity is 50-60wt%.
In step (4), described acid solution is concentration is the hydrochloric acid solution of 1-2mol/L, and described alkali liquor is concentration is the sodium hydroxide solution of 0.5-1mol/L.
In step (5), the solid content of described waterglass is 35-45wt%; Described compressing pressure is 70-80MPa.
In step (6), the heating rate that described first time heats up is 12-16 DEG C/min, the rate of temperature fall of cooling of described first time is 4-8 DEG C/min, and the heating rate that described second time heats up is 10-15 DEG C/min, and the rate of temperature fall of described second time cooling is 5-10 DEG C/min.
The invention have the benefit that
1, energy ceramic of the present invention, multi mineral material is adopted to mix according to applicable proportioning, the energy ceramic formed, under the synergism of above-mentioned each component, the magnetic field energy of applicable intensity can be radiated, match with human magnetic field, biomagnetic effect is produced at inside of human body, play and adjust various uneven with in balanced human or abnormal functional status, increase the circulation of human body vim and vigour, reach unobstructed blood vessels, the pain especially neck, shoulder, waist-leg, arthralgia and human body a variety of causes caused, there is quickly alleviating pain effect; Also advantageously improving body immunity, promote the mediation of body and mind, make people energetic, the advantages such as mood is optimistic, vigorous, and energy ceramic of the present invention has intensity height simultaneously, water absorption rate is low, wearability good, shock resistance is good, market value is big.
2, the preparation method of energy ceramic of the present invention, by using serpentine, olivine, tufa stone, Kaolin, bauxite, red mud as raw material, after the cooling again that first heats up, then carries out shrend, pulverizing, dry obtains the first premix material, using quartz sand, nine eyestone shale, magnetic iron ore, tourmaline, far-infrared ceramic, white clay, Maifanitum as raw material, through acid adjustment, grinding, alkali tune, dry obtain the second premix material, afterwards by described first premix material, described second premix material is mixed homogeneously with remaining raw material, after adding waterglass, repressed molding, dry and obtain dry body, gained dry body heats up through first and lowers the temperature, the energy ceramic finally prepared, various mineral constituent is made to give full play to synergism, the magnetic field energy of applicable intensity can be radiated, match with human magnetic field, biomagnetic effect is produced at inside of human body, it is effectively increased the circulation of human body vim and vigour, reach unobstructed blood vessels, especially to neck, shoulder, waist-leg, the pain that arthralgia and human body a variety of causes cause, there is quickly alleviating pain effect.
Detailed description of the invention
Example below represents 1g with 1 weight portion.
Embodiment 1
Present embodiments provide a kind of energy ceramic, raw material components includes: quartz sand 40 weight portion, nine eyestone shale 50 weight portions, magnetic iron ore 20 weight portion, tourmaline 40 weight portion, far-infrared ceramic 15 weight portion, white clay 25 weight portion, Maifanitum 20 weight portion, kerosene shale ash 25 weight portion, serpentine 15 weight portion, olivine 45 weight portion, tufa stone 15 weight portion, Kaolin 45 weight portion, bauxite 20 weight portion, red mud 45 weight portion, slag micro powder 20 weight portion, and catalyst gives up agent 45 weight portion.
The useless agent of described catalyst is methanol-fueled CLC copper zinc dead catalyst, wherein containing 25wt%CuO, 60wt%ZnO and 10wt%Al2O3, all the other are impurity.
Further, the preparation method of described energy ceramic, comprise the steps:
(1) weigh serpentine, olivine, tufa stone, Kaolin, bauxite, red mud according to above-mentioned weight and be sufficiently mixed, obtaining the first mixed material;
(2) by described first mixed material first with the ramp of 4 DEG C/min to 450 DEG C, insulation 2h, again with the ramp of 2 DEG C/min to 780 DEG C, insulation 1h, it is cooled to 350 DEG C with the speed of 5 DEG C/min again, is incubated 4h, afterwards successively through shrend, pulverizing, dry, obtaining particle diameter is 150 purpose the first premix material, stand-by;
(3) weigh quartz sand, nine eyestone shale, magnetic iron ore, tourmaline, far-infrared ceramic, white clay, Maifanitum and be sufficiently mixed, obtaining the second mixed material;
(4) described second mixed material is first pulverized, obtaining particle diameter is 200 order fine powders, adding water in described fine powder and making concentration is 50wt% serosity, and the pH with the hydrochloric acid solution described serosity of adjustment that concentration is 1mol/L is 4, afterwards by described serosity under 70 DEG C of bath temperatures, with 300r/min speed speed lapping 20min, then to regulate the pH of described serosity with the sodium hydroxide solution that concentration is 0.5mol/L be neutral, spray-dried, obtain the second premix material, stand-by;
(5) described for step (2) the first premix material, described second premix material of step (4) are mixed homogeneously with remaining raw material, obtain the 3rd mixed material, adding solid content in described 3rd mixed material is 35wt% waterglass, the addition of described waterglass is equivalent to the 4wt% of described 3rd mixed material weight, stirring mixing 20min makes its mix homogeneously, compressing through 70MPa, dry obtains dry body;
(6) first carry out being warming up to 980 DEG C for the first time with 12 DEG C/min speed by described for step (3) dry body, insulation 5h, carry out being cooled to 720 DEG C for the first time with the speed of 4 DEG C/min again, be incubated 3h, carry out second time with the speed of 10 DEG C/min more afterwards and be warming up to 1160 DEG C, insulation 8h, it is cooled to 550 DEG C with 5 DEG C/min speed again, is incubated 2h, is cooled to room temperature, through edging, obtain described energy ceramic.
Embodiment 2
Present embodiments provide a kind of energy ceramic, raw material components includes: quartz sand 60 weight portion, nine eyestone shale 30 weight portions, magnetic iron ore 40 weight portion, tourmaline 20 weight portion, far-infrared ceramic 45 weight portion, white clay 15 weight portion, Maifanitum 40 weight portion, kerosene shale ash 15 weight portion, serpentine 45 weight portion, olivine 15 weight portion, tufa stone 45 weight portion, Kaolin 15 weight portion, bauxite 40 weight portion, red mud 15 weight portion, slag micro powder 40 weight portion, and catalyst gives up agent 15 weight portion.
The useless agent of described catalyst is low-temperature conversion copper zinc dead catalyst, wherein containing 65wt%CuO, 30wt%ZnO and 1wt%Al2O3, all the other are impurity.
Further, the preparation method of described energy ceramic, comprise the steps:
(1) weigh serpentine, olivine, tufa stone, Kaolin, bauxite, red mud according to above-mentioned weight and be sufficiently mixed, obtaining the first mixed material;
(2) by described first mixed material first with the ramp of 8 DEG C/min to 550 DEG C, insulation 5h, again with the ramp of 4 DEG C/min to 880 DEG C, insulation 2h, it is cooled to 400 DEG C with the speed of 10 DEG C/min again, is incubated 6h, afterwards successively through shrend, pulverizing, dry, obtaining particle diameter is 200 purpose the first premix material, stand-by;
(3) weigh quartz sand, nine eyestone shale, magnetic iron ore, tourmaline, far-infrared ceramic, white clay, Maifanitum and be sufficiently mixed, obtaining the second mixed material;
(4) described second mixed material is first pulverized, obtaining particle diameter is 300 order fine powders, adding water in described fine powder and making concentration is 60wt% serosity, and the pH with the hydrochloric acid solution described serosity of adjustment that concentration is 2mol/L is 5, afterwards by described serosity under 80 DEG C of bath temperatures, with 500r/min speed speed lapping 30min, then to regulate the pH of described serosity with the sodium hydroxide solution that concentration is 1mol/L be neutral, spray-dried, obtain the second premix material, stand-by;
(5) described for step (2) the first premix material, described second premix material of step (4) are mixed homogeneously with remaining raw material, obtain the 3rd mixed material, adding solid content in described 3rd mixed material is 45wt% waterglass, the addition of described waterglass is equivalent to the 8wt% of described 3rd mixed material weight, stirring mixing 30min makes its mix homogeneously, compressing through 80MPa, dry obtains dry body;
(6) first carry out being warming up to 1060 DEG C for the first time with 16 DEG C/min speed by described for step (3) dry body, insulation 8h, carry out being cooled to 780 DEG C for the first time with the speed of 8 DEG C/min again, be incubated 4h, carry out second time with the speed of 15 DEG C/min more afterwards and be warming up to 1220 DEG C, insulation 12h, it is cooled to 600 DEG C with 10 DEG C/min speed again, is incubated 3h, is cooled to room temperature, through edging, obtain described energy ceramic.
Embodiment 3
Present embodiments provide a kind of energy ceramic, raw material components includes: quartz sand 50 weight portion, nine eyestone shale 40 weight portions, magnetic iron ore 30 weight portion, tourmaline 30 weight portion, far-infrared ceramic 25 weight portion, white clay 20 weight portion, Maifanitum 30 weight portion, kerosene shale ash 20 weight portion, serpentine 30 weight portion, olivine 25 weight portion, tufa stone 30 weight portion, Kaolin 30 weight portion, bauxite 30 weight portion, red mud 28 weight portion, slag micro powder 30 weight portion, and catalyst gives up agent 28 weight portion.
The useless agent of described catalyst is aldehyde Hydrogenation alcohol copper zinc dead catalyst, wherein containing 62wt%CuO, 25wt%ZnO and 10wt%Al2O3, all the other are impurity.
Further, the preparation method of described energy ceramic, comprise the steps:
(1) weigh serpentine, olivine, tufa stone, Kaolin, bauxite, red mud according to above-mentioned weight and be sufficiently mixed, obtaining the first mixed material;
(2) by described first mixed material first with the ramp of 6 DEG C/min to 500 DEG C, insulation 2.5h, again with the ramp of 3 DEG C/min to 800 DEG C, insulation 1.5h, it is cooled to 380 DEG C with the speed of 8 DEG C/min again, is incubated 5h, afterwards successively through shrend, pulverizing, dry, obtaining particle diameter is 180 purpose the first premix material, stand-by;
(3) weigh quartz sand, nine eyestone shale, magnetic iron ore, tourmaline, far-infrared ceramic, white clay, Maifanitum and be sufficiently mixed, obtaining the second mixed material;
(4) described second mixed material is first pulverized, obtaining particle diameter is 250 order fine powders, adding water in described fine powder and making concentration is 55wt% serosity, and the pH with the hydrochloric acid solution described serosity of adjustment that concentration is 1.5mol/L is 4, afterwards by described serosity under 75 DEG C of bath temperatures, with 400r/min speed speed lapping 25min, then to regulate the pH of described serosity with the sodium hydroxide solution that concentration is 0.8mol/L be neutral, spray-dried, obtain the second premix material, stand-by;
(5) described for step (2) the first premix material, described second premix material of step (4) are mixed homogeneously with remaining raw material, obtain the 3rd mixed material, adding solid content in described 3rd mixed material is 40wt% waterglass, the addition of described waterglass is equivalent to the 6wt% of described 3rd mixed material weight, stirring mixing 25min makes its mix homogeneously, compressing through 75MPa, dry obtains dry body;
(6) first carry out being warming up to 1000 DEG C for the first time with 14 DEG C/min speed by described for step (3) dry body, insulation 7h, carry out being cooled to 750 DEG C for the first time with the speed of 6 DEG C/min again, be incubated 3.5h, carry out second time with the speed of 12 DEG C/min more afterwards and be warming up to 1200 DEG C, insulation 10h, it is cooled to 580 DEG C with 8 DEG C/min speed again, is incubated 2.5h, is cooled to room temperature, through edging, obtain described energy ceramic.
Embodiment 4
Present embodiments provide a kind of energy ceramic, raw material components includes: quartz sand 50 weight portion, nine eyestone shale 40 weight portions, magnetic iron ore 30 weight portion, tourmaline 30 weight portion, far-infrared ceramic 25 weight portion, white clay 20 weight portion, Maifanitum 30 weight portion, kerosene shale ash 20 weight portion, serpentine 30 weight portion, olivine 25 weight portion, tufa stone 30 weight portion, Kaolin 30 weight portion, bauxite 30 weight portion, red mud 28 weight portion, slag micro powder 30 weight portion, and catalyst gives up agent 28 weight portion.
The useless agent of described catalyst is aldehyde Hydrogenation alcohol copper zinc dead catalyst, wherein containing 62wt%CuO, 25wt%ZnO and 10wt%Al2O3, all the other are impurity.
Further, the preparation method of described energy ceramic, comprise the steps:
(1) weigh serpentine, olivine, tufa stone, Kaolin, bauxite, red mud according to above-mentioned weight and be sufficiently mixed, obtaining the first mixed material;
(2) by described first mixed material first with the ramp of 6 DEG C/min to 500 DEG C, insulation 2.5h, again with the ramp of 3 DEG C/min to 800 DEG C, insulation 1.5h, it is cooled to 380 DEG C with the speed of 8 DEG C/min again, is incubated 5h, afterwards successively through shrend, pulverizing, dry, obtaining particle diameter is 200 purpose the first premix material, stand-by;
(3) weigh quartz sand, nine eyestone shale, magnetic iron ore, tourmaline, far-infrared ceramic, white clay, Maifanitum and be sufficiently mixed, obtaining the second mixed material;
(4) described second mixed material is first pulverized, obtaining particle diameter is 300 order fine powders, adding water in described fine powder and making concentration is 55wt% serosity, and the pH with the hydrochloric acid solution described serosity of adjustment that concentration is 2mol/L is 4, afterwards by described serosity under 75 DEG C of bath temperatures, with 400r/min speed speed lapping 25min, then to regulate the pH of described serosity with the sodium hydroxide solution that concentration is 1mol/L be neutral, spray-dried, obtain the second premix material, stand-by;
(5) described for step (2) the first premix material, described second premix material of step (4) are mixed homogeneously with remaining raw material, obtain the 3rd mixed material, adding solid content in described 3rd mixed material is 40wt% waterglass, the addition of described waterglass is equivalent to the 6wt% of described 3rd mixed material weight, stirring mixing 25min makes its mix homogeneously, compressing through 80MPa, dry obtains dry body;
(6) first carry out being warming up to 1000 DEG C for the first time with 14 DEG C/min speed by described for step (3) dry body, insulation 7h, carry out being cooled to 750 DEG C for the first time with the speed of 6 DEG C/min again, be incubated 4h, carry out second time with the speed of 12 DEG C/min more afterwards and be warming up to 1200 DEG C, insulation 10h, it is cooled to 580 DEG C with 8 DEG C/min speed again, is incubated 3h, is cooled to room temperature, through edging, obtain described energy ceramic.
Embodiment 5
Present embodiments provide a kind of energy ceramic, raw material components includes: quartz sand 60 weight portion, nine eyestone shale 40 weight portions, magnetic iron ore 30 weight portion, tourmaline 30 weight portion, far-infrared ceramic 25 weight portion, white clay 20 weight portion, Maifanitum 30 weight portion, kerosene shale ash 20 weight portion, serpentine 30 weight portion, olivine 25 weight portion, tufa stone 30 weight portion, Kaolin 30 weight portion, bauxite 30 weight portion, red mud 28 weight portion, slag micro powder 30 weight portion, and catalyst gives up agent 28 weight portion.
The useless agent of described catalyst be methanol-fueled CLC copper zinc dead catalyst, low-temperature conversion copper zinc dead catalyst, aldehyde Hydrogenation alcohol copper zinc dead catalyst according to the mass ratio 1:1:1 mixture formed, containing 45wt%CuO, 45wt%ZnO and 5wt%Al in mixture2O3, all the other are impurity.
Further, the preparation method of described energy ceramic, comprise the steps:
(1) weigh serpentine, olivine, tufa stone, Kaolin, bauxite, red mud according to above-mentioned weight and be sufficiently mixed, obtaining the first mixed material;
(2) by described first mixed material first with the ramp of 6 DEG C/min to 500 DEG C, insulation 2.5h, again with the ramp of 3 DEG C/min to 800 DEG C, insulation 1.5h, it is cooled to 380 DEG C with the speed of 8 DEG C/min again, is incubated 5h, afterwards successively through shrend, pulverizing, dry, obtaining particle diameter is 180 purpose the first premix material, stand-by;
(3) weigh quartz sand, nine eyestone shale, magnetic iron ore, tourmaline, far-infrared ceramic, white clay, Maifanitum and be sufficiently mixed, obtaining the second mixed material;
(4) described second mixed material is first pulverized, obtaining particle diameter is 250 order fine powders, adding water in described fine powder and making concentration is 55wt% serosity, and the pH with the hydrochloric acid solution described serosity of adjustment that concentration is 1.5mol/L is 4, afterwards by described serosity under 75 DEG C of bath temperatures, with 400r/min speed speed lapping 25min, then to regulate the pH of described serosity with the sodium hydroxide solution that concentration is 0.8mol/L be neutral, spray-dried, obtain the second premix material, stand-by;
(5) described for step (2) the first premix material, described second premix material of step (4) are mixed homogeneously with remaining raw material, obtain the 3rd mixed material, adding solid content in described 3rd mixed material is 40wt% waterglass, the addition of described waterglass is equivalent to the 6wt% of described 3rd mixed material weight, stirring mixing 25min makes its mix homogeneously, compressing through 75MPa, dry obtains dry body;
(6) first carry out being warming up to 1000 DEG C for the first time with 14 DEG C/min speed by described for step (3) dry body, insulation 7h, carry out being cooled to 750 DEG C for the first time with the speed of 6 DEG C/min again, be incubated 3.5h, carry out second time with the speed of 12 DEG C/min more afterwards and be warming up to 1200 DEG C, insulation 10h, it is cooled to 580 DEG C with 8 DEG C/min speed again, is incubated 2.5h, is cooled to room temperature, through edging, obtain described energy ceramic.
Embodiment 3 clinical verification
The present inventor by clinical 700 example patients are carried out clinical observation treatment, age 20-65 year, including cervical spondylosis, scapulohumeral periarthritis, prolapse of lumbar intervertebral disc, rheumatic arthritis, traumatic injury, lumbago and skelalgia, acute psoas strain patient, each type patient 100 people.
Therapeutic Method: every day 1 time, each 30min, 10 days course for the treatment of, embodiment 3 energy ceramic is attached directly to body foci position.
Efficacy assessment standard:
Cure: the Clinical symptom and sign such as neck, shoulder, waist, lower limb place pain, swelling, numbness, function limitation disappear, and exercise recovery is normal.
Effective: clinical symptoms takes a turn for the better or major part disappears.
Invalid: symptom and sign is not improved.
3 course of therapy effects:
| Cure | Cure rate | Effectively | Invalid | Total effective rate | |
| Cervical spondylosis | 58 | 58% | 38 | 4 | 96% |
| Scapulohumeral periarthritis | 62 | 62% | 34 | 4 | 96% |
| Prolapse of lumbar intervertebral disc | 30 | 30% | 60 | 10 | 90% |
| Rheumatic arthritis | 42 | 42% | 53 | 5 | 95% |
| Traumatic injury | 78 | 78% | 19 | 3 | 97% |
| Lumbago and skelalgia | 73 | 73% | 24 | 3 | 97% |
| Acute psoas strains | 82 | 82% | 16 | 2 | 98% |
The present invention is not limited to above-mentioned preferred forms; anyone can draw other various forms of products under the enlightenment of the present invention; no matter but in its shape or structure, do any change; every have same or like with the application like technical scheme, all fall within protection scope of the present invention.
Claims (10)
1. an energy ceramic, it is characterized in that, raw material components includes: quartz sand 40-60 weight portion, nine eyestone shale 30-50 weight portions, magnetic iron ore 20-40 weight portion, tourmaline 20-40 weight portion, far-infrared ceramic 15-45 weight portion, white clay 15-25 weight portion, Maifanitum 20-40 weight portion, kerosene shale ash 15-25 weight portion, serpentine 15-45 weight portion, olivine 15-45 weight portion, tufa stone 15-45 weight portion, Kaolin 15-45 weight portion, bauxite 20-40 weight portion, red mud 15-45 weight portion, slag micro powder 20-40 weight portion, catalyst gives up agent 15-45 weight portion.
2. energy ceramic according to claim 1, it is characterized in that, raw material components includes: quartz sand 50 weight portion, nine eyestone shale 40 weight portions, magnetic iron ore 30 weight portion, tourmaline 30 weight portion, far-infrared ceramic 25 weight portion, white clay 20 weight portion, Maifanitum 30 weight portion, kerosene shale ash 20 weight portion, serpentine 30 weight portion, olivine 25 weight portion, tufa stone 30 weight portion, Kaolin 30 weight portion, bauxite 30 weight portion, red mud 28 weight portion, slag micro powder 30 weight portion, and catalyst gives up agent 28 weight portion.
3. energy ceramic according to claim 1, it is characterised in that the useless agent of described catalyst is one or more in methanol-fueled CLC copper zinc dead catalyst, low-temperature conversion copper zinc dead catalyst, aldehyde Hydrogenation alcohol copper zinc dead catalyst.
4. the method for the energy ceramic prepared described in any one of claim 1-3, it is characterised in that comprise the steps:
(1) weigh serpentine, olivine, tufa stone, Kaolin, bauxite, red mud and be sufficiently mixed, obtaining the first mixed material;
(2) described first mixed material is first carried out being warming up to 780-880 DEG C, be incubated 1-2h, then be cooled to 350-400 DEG C, be incubated 4-6h, afterwards successively through shrend, pulverizing, dry, obtain the first premix material, stand-by;
(3) weigh quartz sand, nine eyestone shale, magnetic iron ore, tourmaline, far-infrared ceramic, white clay, Maifanitum and be sufficiently mixed, obtaining the second mixed material;
(4) described second mixed material is first pulverized, obtain fine powder, add water in described fine powder and make serosity, and the pH with the acid solution described serosity of adjustment is 4-5, afterwards described serosity is ground at 70-80 DEG C of temperature 20-30min, then the pH with the alkali liquor described serosity of adjustment is neutral, spray-dried, obtain the second premix material, stand-by;
(5) described for step (2) the first premix material, described second premix material of step (4) are mixed homogeneously with remaining raw material, obtain the 3rd mixed material, waterglass is added in described 3rd mixed material, the addition of described waterglass is equivalent to the 4-8wt% of described 3rd mixed material weight, it is uniformly mixed, repressed molding, dry obtains dry body;
(6) first carry out step (3) described dry body being warming up to 980-1060 DEG C for the first time, insulation 5-8h, carry out again being cooled to 720-780 DEG C for the first time, be incubated 3-4h, carry out second time afterwards again and be warming up to 1160-1220 DEG C, insulation 8-12h, it is cooled to 550-600 DEG C again, is incubated 2-3h, is cooled to room temperature, through edging, obtain described energy ceramic.
5. the preparation method of energy ceramic according to claim 4, it is characterized in that, in step (2), described temperature-rise period is: first by described first mixed material with the ramp of 4-8 DEG C/min to 450-550 DEG C, insulation 2-5h, then with the ramp of 2-4 DEG C/min to 780-880 DEG C;
The rate of temperature fall of described temperature-fall period is 5-10 DEG C/min.
6. the preparation method of energy ceramic according to claim 4, it is characterised in that in step (2), the particle diameter of described first premix material is 150-200 order.
7. the preparation method of energy ceramic according to claim 4, it is characterised in that in step (4), the particle diameter of described fine powder is 200-300 order, and the concentration of described serosity is 50-60wt%.
8. the preparation method of energy ceramic according to claim 4, it is characterised in that in step (4), described acid solution is concentration is the hydrochloric acid solution of 1-2mol/L, and described alkali liquor is concentration is the sodium hydroxide solution of 0.5-1mol/L.
9. the preparation method of energy ceramic according to claim 4, it is characterised in that in step (4), in step (5), the solid content of described waterglass is 35-45wt%; Described compressing pressure is 70-80MPa.
10. the preparation method of energy ceramic according to claim 4, it is characterized in that, in step (6), the heating rate that described first time heats up is 12-16 DEG C/min, the rate of temperature fall of cooling of described first time is 4-8 DEG C/min, the heating rate that described second time heats up is 10-15 DEG C/min, and the rate of temperature fall of described second time cooling is 5-10 DEG C/min.
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| CN107500733A (en) * | 2017-09-22 | 2017-12-22 | 苏州瓷气时代净化设备有限公司 | A kind of preparation method of durable health ceramic |
| CN107500739A (en) * | 2017-09-22 | 2017-12-22 | 苏州瓷气时代净化设备有限公司 | A kind of healthcare function ceramic |
| CN110451913A (en) * | 2019-08-12 | 2019-11-15 | 山东木齐健康科技有限公司 | Multicolored graphene rice crystalline substance porcelain moxibustion functional material and its preparation method and application |
| CN110540417A (en) * | 2019-09-10 | 2019-12-06 | 孙昌印 | Energy stone capable of releasing far infrared rays and preparation method and application thereof |
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