CN103896558A - Preparation method of infrared ceramic vacuum cup and product prepared by same - Google Patents

Preparation method of infrared ceramic vacuum cup and product prepared by same Download PDF

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Publication number
CN103896558A
CN103896558A CN201410088764.0A CN201410088764A CN103896558A CN 103896558 A CN103896558 A CN 103896558A CN 201410088764 A CN201410088764 A CN 201410088764A CN 103896558 A CN103896558 A CN 103896558A
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glaze
preparation
blank
oxide
mud
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CN103896558B (en
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肖杨
胡飞
谢庚
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GANGPENG INDUSTRY Co Ltd HUNAN PROV
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GANGPENG INDUSTRY Co Ltd HUNAN PROV
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Abstract

The invention relates to a preparation method of an infrared ceramic vacuum cup and a product prepared by the same. A formula of a blank comprises the raw materials in parts by weight: 10-30% of Longyan cleansing mud, 10-30% of Chenzhou mud, 15-30% of Yunnan sand, 15-30% of potassium feldspar, 5-10% of medical stone, 0.5-5% of titanium oxide, 2-10% of zirconium silicate, 0.5-3% of manganese dioxide and 0.2-1% of yttrium oxide. A formula of glaze comprises the raw materials in parts by weight: 20-40% of potassium feldspar, 5-15% of sodium feldspar, 5-15% of kaolin, 20-40% of quartz, 10-30% of calcite, 1-5% of talc, 1-5% of zinc oxide, 1-5% of titanium oxide, 2-5% of manganese dioxide, 5-15% of zirconium silicate, 1-5% of ferric oxide and 0.2-1% of yttrium oxide. The product with a good health care function is obtained by the steps of preparing the blank and the glaze, forming, drying, biscuiting, glazing and firing glaze and has broad application prospect.

Description

A kind of preparation method of infra-red china thermos cup and the product making thereof
Technical field
The invention belongs to ceramic (pottery) field, be specifically related to a kind of preparation method of infra-red china thermos cup and the product making thereof.
Background technology
The vibrational frequency of far infrared rays and human inner cell's molecule approaches, can cause the resonance of atom and the molecule of human body cell, absorb frictional heat between molecule by sympathetic response and form thermal response, promote subcutaneous deep temperature rise, and make Marjoram Extract, promote and improve blood circulation, strengthen metabolism, be conducive to remove blood vessel and hoard objectionable impurities in thing and body, improve immune function of human body, there is good human body heath care function.Can emitting far-infrared material be inorganic materials mostly, this be easily to form defect because inorganic materials is inner, as doped Ti in the crystalline phase of mullite, trichroite 4+, Mg 2+, Y 3+, Pd 3+, Ni 2+, Fe 3+, Zr 4+, Ti 4+after plasma, molecular vibration is asymmetric and launch far infrared rays.
In CN102070324A, prepare a kind of far-infrared ceramic ball, this Ceramic Balls can give off far infrared rays, kills the harmful microorganisms such as the intestinal bacteria in water.Patent CN1027365C prepares far-infrared ceramic powder, and then adds in various vessel, clothes, comes emitting far-infraredly by far-infrared ceramic powder, can play a role in health care.Chinese patent CN101849781 joins Tourmaline haydite ball in the interlayer of thermos cup, but Tourmaline haydite ball transmitting far-infrared functional a little less than, low to the activity performance of water, but up to the present also far infrared health care technology is not applied to the report in ceramic cup.
Summary of the invention
The technical problem to be solved in the present invention be to provide a kind of to water have mobilizing function, there is good nourishing function, raw materials cost is cheap, the preparation method of the simple infra-red china thermos cup of production technique and the product making thereof.
For solving above technical problem, technical scheme of the present invention is: a kind of preparation method of infra-red china thermos cup, adopt raw mineral materials and industrial chemicals, and the weight percent of its blank and glaze formula consists of:
Blank: mud 10~30%, Chenzhou mud 10~30%, Yunnan sand 15~30%, potassium felspar sand 15~30%, medical stone 5~10%, titanium oxide 0.5~5%, zirconium silicate 2~10%, Manganse Dioxide 0.5~3%, yttrium oxide 0.2~1% are washed in Longyan;
Glaze: potassium felspar sand 20~40%, albite 5~15%, kaolin 5~15%, quartz 20~40%, calcite 10~30%, talcum 1~5%, zinc oxide 1~5%, titanium oxide 1~5%, Manganse Dioxide 2~5%, zirconium silicate 5~15%, ferric oxide 1~5%, yttrium oxide 0.2~1%;
Burn and obtain goods through blank and glaze preparation, moulding, dry, base substrate biscuiting, glazing, dry, medium temperature glaze, wherein base substrate biscuiting temperature range is: 700~1100 ℃, it is that 1280 ℃, firing time are 8~10h that medium temperature glaze burns temperature.
The preparation technology of described blank is: mix by blank formulation raw materials weighing, adding weight percent is that the water glass of 0.1~0.4% tripoly phosphate sodium STPP and 0.2~0.8% is as thinner, then pack ball milling in ball-grinding machine into, going out to grind pug proportion is 1.58~1.65g/cm 3, then through the old blank of making.
The preparation technology of described glaze is: after closing evenly by glaze formula raw materials weighing, adding weight percent is that the tripoly phosphate sodium STPP of 0.3~0.8% carboxymethyl cellulose and 0.2~0.6% is as additive, then pack ball milling in ball-grinding machine into, going out to grind glaze proportion is 1.55~1.65g/cm 3.
Described zinc oxide, aluminum oxide, talcum need first to pass through pre-burning before using, and calcining temperature is 1200 ℃.
The mass percent of described glaze chemical composition is as follows: Al 2o 36~10%, SiO 264~68%, K 2o 0.5~5%, Na 2o 0.2~3%, MgO 0.1~2%, CaO 0.4~15%, ZrO 20.1~8%, ZnO 0.05~5%, TiO 21~5%, Mn0 22~5%, Y 2o 30.2~1%.
The infra-red china thermos cup product that above-mentioned preparation method makes, is characterized in that: the normal direction whole radiation rate of described product is 0.90~0.95.
The present invention adopts natural mineral raw and industrial pure material to prepare a kind of far-infrared ceramic thermos cup, this infra-red china thermos cup not only can activate the water in thermos cup, can improve again microcirculation in human body simultaneously, strengthen metabolism, improve human immunological competence, there is good nourishing function, therefore there are wide market outlook.
Embodiment
Implementation column one:
A kind of far-infrared ceramic thermos cup, takes blank: mud 15% is washed in Longyan, Chenzhou mud 17% by mass percentage, Yunnan sand 25%, potassium felspar sand 20%, medical stone 8%, titanium oxide 5%, zirconium silicate 8%, Manganse Dioxide 1.2%, yttrium oxide 0.8% adds 0.2% tripoly phosphate sodium STPP and 0.5% water glass in blank raw material, mixing and ball milling, adjustment mud balance is 1.60g/cm 3, after mud is old, casting obtains base substrate, and this base substrate passes through biscuiting in advance, and biscuiting temperature is 1000 ℃;
Take by mass percentage glaze: potassium felspar sand 20%, albite 8%, kaolin 5%, quartz 27.5%, calcite 15%, talcum 3%, zinc oxide 1%, titanium oxide 5%, manganese oxide 5%, zirconium silicate 8%, ferric oxide 1.5%, yttrium oxide 1%, the mass percent of its chemical composition is: Al 2o 38.6%, SiO 265%, K 2o 2.5%, Na 2o 1%, MgO 1%, CaO 9%, ZrO 25%, ZnO 1%, TiO 22%, Mn0 24%, Y 2o 30.9%, in glaze, add 0.5% carboxymethyl cellulose and 0.3% tripoly phosphate sodium STPP, mixing and ball milling, adjusting glaze proportion is 1.58g/cm 3, then, in the thermal-insulation ceramic cup capable ectonexine glazing of biscuiting, dry, burning till at 1280 ℃, firing time is 9h.
The sample preparing is carried out to far infrared transmission performance test, and normal direction whole radiation rate is 0.91.
Implementation column two:
A kind of far-infrared ceramic thermos cup, take by mass percentage blank: mud 13%, Chenzhou mud 16%, Yunnan sand 23%, potassium felspar sand 25%, medical stone 10%, titanium oxide 5%, zirconium silicate 6%, Manganse Dioxide 1.3%, yttrium oxide 0.7% are washed in Longyan, in blank raw material, add 0.1% tripoly phosphate sodium STPP and 0.4% water glass.Mixing and ball milling, adjustment mud balance is 1.62g/cm 3, after mud is old, casting obtains base substrate, and this base substrate passes through biscuiting in advance, and biscuiting temperature is 1000 ℃;
Take by mass percentage glaze: potassium felspar sand 35%, albite 5%, kaolin 9%, quartz 20%, calcite 10%, talcum 2%, zinc oxide 3%, titanium oxide 4%, manganese oxide 3%, zirconium silicate 7%, ferric oxide 1.2%, yttrium oxide 0.8%, the mass percent of its chemical composition is: Al 2o 37.68%, SiO 266%, K 2o 2.5%, Na 2o 1.2%, MgO 0.9%, CaO 6%, ZrO 25%, ZnO 3%, TiO 24%, Mn0 23%, Y 2o 30.72%, in glaze, add 0.4% carboxymethyl cellulose and 0.3% tripoly phosphate sodium STPP.Mixing and ball milling, adjusts glaze proportion at 1.60g/cm 3, then, in the thermal-insulation ceramic cup capable ectonexine glazing of biscuiting, dry, burning till at 1280 ℃, firing time is 8h.
The sample preparing is carried out to far infrared transmission performance test, and normal direction whole radiation rate is 0.92.
Implementation column three:
A kind of far-infrared ceramic thermos cup, take by mass percentage blank: mud 30%, Chenzhou mud 11%, Yunnan sand 17%, potassium felspar sand 28%, medical stone 6%, titanium oxide 2%, zirconium silicate 3%, Manganse Dioxide 2.3%, yttrium oxide 0.7% are washed in Longyan, in blank raw material, add 0.2% tripoly phosphate sodium STPP and 0.7% water glass.Mixing and ball milling, adjustment mud balance is 1.64g/cm 3, after mud is old, casting obtains base substrate, and this base substrate passes through biscuiting in advance, and biscuiting temperature is 1000 ℃;
Take by mass percentage glaze: potassium felspar sand 20%, albite 5%, kaolin 13%, quartz 20%, calcite 15.7%, talcum 3%, zinc oxide 4%, titanium oxide 2%, manganese oxide 2%, zirconium silicate 12%, ferric oxide 3%, yttrium oxide 0.3%, the mass percent of its chemical composition is: Al 2o 39%, SiO 268%, K 2o 2.5%, Na 2o 2.2%, MgO 1.9%, CaO 6%, ZrO 21.68%, ZnO 1%, TiO 24%, Mn0 23.5%, Y 2o 30.22%, in glaze, add 0.4% carboxymethyl cellulose and 0.3% tripoly phosphate sodium STPP.Mixing and ball milling, adjusts glaze proportion at 1.64g/cm 3, then, in the thermal-insulation ceramic cup capable ectonexine glazing of biscuiting, dry, burning till at 1280 ℃, firing time is 8h.
The sample preparing is carried out to far infrared transmission performance test, and normal direction whole radiation rate is 0.95.

Claims (6)

1. a preparation method for infra-red china thermos cup, adopts raw mineral materials and industrial chemicals, and the weight percent of its blank and glaze formula consists of:
Blank: mud 10~30%, Chenzhou mud 10~30%, Yunnan sand 15~30%, potassium felspar sand 15~30%, medical stone 5~10%, titanium oxide 0.5~5%, zirconium silicate 2~10%, Manganse Dioxide 0.5~3%, yttrium oxide 0.2~1% are washed in Longyan;
Glaze: potassium felspar sand 20~40%, albite 5~15%, kaolin 5~15%, quartz 20~40%, calcite 10~30%, talcum 1~5%, zinc oxide 1~5%, titanium oxide 1~5%, Manganse Dioxide 2~5%, zirconium silicate 5~15%, ferric oxide 1~5%, yttrium oxide 0.2~1%;
Burn and obtain goods through blank and glaze preparation, moulding, dry, base substrate biscuiting, glazing, dry, medium temperature glaze, wherein base substrate biscuiting temperature range is: 700~1100 ℃, it is that 1280 ℃, firing time are 8~10h that medium temperature glaze burns temperature.
2. preparation method according to claim 1, it is characterized in that: the preparation technology of described blank is: mix by blank formulation raw materials weighing, adding weight percent is that the water glass of 0.1~0.4% tripoly phosphate sodium STPP and 0.2~0.8% is as thinner, then pack ball milling in ball-grinding machine into, going out to grind pug proportion is 1.58~1.65g/cm 3, then through the old blank of making.
3. preparation method according to claim 1, it is characterized in that: the preparation technology of described glaze is: after closing evenly by glaze formula raw materials weighing, adding weight percent is that the tripoly phosphate sodium STPP of 0.3~0.8% carboxymethyl cellulose and 0.2~0.6% is as additive, then pack ball milling in ball-grinding machine into, going out to grind glaze proportion is 1.55~1.65g/cm 3.
4. preparation method according to claim 1, is characterized in that: described zinc oxide, aluminum oxide, talcum need first to pass through pre-burning before using, and calcining temperature is 1200 ℃.
5. preparation method according to claim 1, is characterized in that: the mass percent of described glaze chemical composition is as follows: Al 2o 36~10%, SiO 264~68%, K 2o 0.5~5%, Na 2o 0.2~3%, MgO 0.1~2%, CaO 0.4~15%, ZrO 20.1~8%, ZnO 0.05~5%, TiO 21~5%, Mn0 22~5%, Y 2o 30.2~1%.
6. the infra-red china thermos cup product making according to the arbitrary described preparation method of claim 1-5, is characterized in that: the normal direction whole radiation rate of described product is 0.90~0.95.
CN201410088764.0A 2014-03-12 2014-03-12 Preparation method of infrared ceramic vacuum cup and product prepared by same Active CN103896558B (en)

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105344021A (en) * 2015-11-07 2016-02-24 德化均能手造陶瓷有限公司 Optical wafer for activating blood and dredging collaterals
CN106277788A (en) * 2016-08-23 2017-01-04 宜兴市方卫明均陶艺术研究所 A kind of enamel glaze and preparation method thereof
CN107056263A (en) * 2017-04-27 2017-08-18 湖南港鹏实业有限公司 A kind of preparation method of middle temperature feldspathic bone china
CN110204205A (en) * 2019-05-23 2019-09-06 醴陵陶润实业发展有限公司 Crude pottery and preparation method thereof
CN110655382A (en) * 2019-08-02 2020-01-07 景德镇御腾瓷器有限公司 Preparation method of health-care ball with high far infrared radiance
CN111333430A (en) * 2020-05-19 2020-06-26 佛山市东鹏陶瓷发展有限公司 Deodorizing glaze and preparation method of glazed tile using same
CN111548010A (en) * 2020-05-06 2020-08-18 佛山科学技术学院 Antibacterial aromatic ceramic glaze
CN113061055A (en) * 2021-03-25 2021-07-02 景德镇陶瓷大学 Antibacterial ceramic product and preparation method and application thereof
CN113416056A (en) * 2021-02-02 2021-09-21 国启艾福佳健康科技(山东)有限公司 Ceramic energy storage tube and preparation method thereof
CN113816772A (en) * 2021-09-27 2021-12-21 清远纳福娜陶瓷有限公司 Preparation method of cockroach-repelling ceramic tile and prepared cockroach-repelling ceramic tile

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CN1837140A (en) * 2006-03-31 2006-09-27 潮州市波士发陶瓷制作有限公司 Reinforced osseous porcelain and process for producing same
KR20120037293A (en) * 2010-10-11 2012-04-19 명지대학교 산학협력단 Glaze composition for ceramic ware comprising ashes from the excrements of earthworm and preparation method thereof
CN103408328A (en) * 2013-07-31 2013-11-27 蔡焕宜 Ceramic glaze and preparation method thereof
CN103467134A (en) * 2012-06-06 2013-12-25 湖南泰鑫瓷业有限公司 Preparation method of beige high brightness metal glaze
CN103553565A (en) * 2013-10-22 2014-02-05 马仁水 Medical stone ceramic product and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1837140A (en) * 2006-03-31 2006-09-27 潮州市波士发陶瓷制作有限公司 Reinforced osseous porcelain and process for producing same
KR20120037293A (en) * 2010-10-11 2012-04-19 명지대학교 산학협력단 Glaze composition for ceramic ware comprising ashes from the excrements of earthworm and preparation method thereof
CN103467134A (en) * 2012-06-06 2013-12-25 湖南泰鑫瓷业有限公司 Preparation method of beige high brightness metal glaze
CN103408328A (en) * 2013-07-31 2013-11-27 蔡焕宜 Ceramic glaze and preparation method thereof
CN103553565A (en) * 2013-10-22 2014-02-05 马仁水 Medical stone ceramic product and preparation method thereof

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105344021A (en) * 2015-11-07 2016-02-24 德化均能手造陶瓷有限公司 Optical wafer for activating blood and dredging collaterals
CN106277788A (en) * 2016-08-23 2017-01-04 宜兴市方卫明均陶艺术研究所 A kind of enamel glaze and preparation method thereof
CN106277788B (en) * 2016-08-23 2018-11-30 宜兴市方卫明均陶艺术研究所 A kind of enamel glaze and preparation method thereof
CN107056263A (en) * 2017-04-27 2017-08-18 湖南港鹏实业有限公司 A kind of preparation method of middle temperature feldspathic bone china
CN110204205A (en) * 2019-05-23 2019-09-06 醴陵陶润实业发展有限公司 Crude pottery and preparation method thereof
CN110655382A (en) * 2019-08-02 2020-01-07 景德镇御腾瓷器有限公司 Preparation method of health-care ball with high far infrared radiance
CN111548010A (en) * 2020-05-06 2020-08-18 佛山科学技术学院 Antibacterial aromatic ceramic glaze
CN111333430A (en) * 2020-05-19 2020-06-26 佛山市东鹏陶瓷发展有限公司 Deodorizing glaze and preparation method of glazed tile using same
CN113416056A (en) * 2021-02-02 2021-09-21 国启艾福佳健康科技(山东)有限公司 Ceramic energy storage tube and preparation method thereof
CN113061055A (en) * 2021-03-25 2021-07-02 景德镇陶瓷大学 Antibacterial ceramic product and preparation method and application thereof
CN113816772A (en) * 2021-09-27 2021-12-21 清远纳福娜陶瓷有限公司 Preparation method of cockroach-repelling ceramic tile and prepared cockroach-repelling ceramic tile

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